TiO2 photocatalytic reactions for organic synthesis have recently been the subject of many reports. The choice and reaction conditions of catalysts are very important in the phenol hydroxylation using H2O2 as oxidant. In this study, a new type of photocatalyst based on silicate (Fe-Al-silicate) was prepared and characterized with a goal to effective utilizing in photocatalytic organic synthesis of dihydroxybenzenes from phenol...