Catalyst characterisation, kinetic and thermodynamic measurements

Pulse Chemisorption TPD, TPO, TPR, TP-Reaction Catalyst Screening On-Line continuous product analysis Metal Surface Area Active Surface Area Reaction Kinetics Mechanisms of Surface Reactions Heats of Adsorption

The CATLAB-PCS microreactor module for the combined roles of catalyst characterisation and rapid, reproducible screening of catalyst activity, featuring:

• Fast response, low thermal mass furnace with integrated air-cooling.
• 1-20 °C / min heating rates up to 1000 °C.
• Hiden’s unique interchangeable Catalyst Cartridge System.
• Close-coupled hotzone evolved species probe & direct QIC inlet for <500ms response.
• ‘In-Bed’ thermocouple for direct catalyst temperature measurement.
• Automatic 2-8 gas stream manifold or combined gas / vapour manifold.
• Independent Mass Flow control of each channel at 3-100 ml / min.
• Corrosion resistant manifold configurations also available.
• Seamless on-line, real-time studies with data acquisition and PC analysis.
• Air thermostat and trace heating to minimise condensation of liquid feeds / products.
• Shut-off / bypass flow configuration to seal reactor and gas sampling port.

CATLAB Systems - Microreactor for Catalysis Studies and Thermal Analysis (291K)

Mass Spectrometers for Catalysis and Thermal Analysis (861K)

QIC Series Gas Analysers - Real-time Gas Analysis Systems (152K)

 A TPD-MS Study of Novel Hydrogen Storage Materials (143K)

 Application of Pd Catalysts for the Hydrogenation of Nitriles (215K)

 Gas Phase Hydrogenation of 1,3-Pentadine, an FTIR Study (603K)

 New Mesoporous Silica Supported Nickel Catalysts for Biomass Conversion (1568KB)

 Plasma Modification of Catalysts Using a Dielectric Barrier Discharge (857KB)

 Plasma Modified Nickel Catalysts for Biomass Conversion (509KB)

 Reaction of Steam and Methane over Novel YSZ-LaB6 Composities and Nickel-YSZ Cermets (474KB)

 Reaction Studies of a Combined Plasma Catalyst Reactor (812K)

 An Intergrated Microreactor MS for Catalyst Characterisation and Evaluation (4844K)

 CATLAB Dispersion Measurement by CO Pulse Chemisorption (470K)

 NOx Detection. The Detection of NO and NO2 using the HPR-20 (158KB)

 Temperature Programmed Reduction with the QIC Series (329K)

Technical Information

 CATLAB Sample Size (428K)

 CATLAB Schematic (284K)

 CATLAB Software - Automated Experimental Control (818K)

 Temperature Programmed Techniques with the Hiden CATLAB (509K)

Academic References

 CATALYSIS - Selected Academic References (413K)

 CATLAB - Selected Academic References (121K)